Isomerization of A Cyclic Ketone Chemistry Lab

Isomerization of A Cyclic Ketone Chemistry Lab

 
Hi there,



All the required documents for this assignment is uploaded down here please read them all to be able to do work



Note: if you by any chance have done this assignment before, please do not copy or use the exact same words that you did before as it happened to me before.



all the experiment questions and instruction should be in files i uploaded and if you have any questions do not heistate to ask.



Thank you.



Videos of Experiment 41:



1) Experiment 41 synthesis and isolation of product (Links to an external site.)



2) IR determination of product4 attachmentsSlide 1 of 4




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UNFORMATTED ATTACHMENT PREVIEW



Experiment 41: Isomerization of a Cyclic Ketone (from Lehman text, 2nd edition) Goal: To determine the identity of the product formed from the acid-catalyzed isomerization of carvone by analyzing the product’s NMR and IR spectra. The Reaction: O H2SO4 C10H14O carvone * Read the entire lab experiment in the Lehman text (pages 354 – 360) to obtain a more complete understanding of Experiment 41 (Note: The full experiment is provided on Canvas). Procedure Notes: *Note: We will using the Standard Scale procedure (You can ignore the microscale procedure). Reaction: • • • • Combine carvone, H2SO4 and magnetic stir bar in a 50 mL round-bottom flask and set up apparatus for heating under reflux. Use a H2O bath (with boiling chips) to heat your reaction mixture. Make sure to maintain vigorous stirring throughout the reaction period. Start timing



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